None: 3,5-dichlorobenzylamine ( 153 mg , 0.87 mmol ) 
None: aluminum chloride ( 27 mg , 0.20 mmol ) 
None: toluene ( 8 mL ) 
None: nitrogen 
None: NaHCO3 solution 
None: ethylenediaminetetraacetic acid ( 1 g , 3.4 mmol ) 
None: chloroform 
None: Na2SO4 
